Structure

wg3

WG3

WG3 Leaders

Lead

Prof 
Wolfgang Fritzsche
WG3 leader
Liebniz Institute of Photonic Technology
Prof 
Moritz Bigalke
WG3 co-leader
Technical University of Darmstadt

WG3

Description

The objectives of WG3 are to (1) understand the potential of the tools available for the analysis, (2) to help European and developing countries to assess harmonized methods, and (3) to facilitate and encourage access to EU research infrastructures and facilities. The planned activities will include the establishment of guidelines and standard operating procedures for established analytical approaches such as optical/fluorescence microscopy, vibrational spectroscopy (Fourier transform infrared and Raman spectroscopy), and thermal methods (e.g., differential scanning calorimetry or pyrolysis gas chromatography mass spectrometry). For the established techniques, special emphasis will be placed on standardized methods with a higher throughput, in order to realize a statistically relevant characterization of samples. On the other hand, novel analytical approaches having the potential to detect as well as identify plastic particles of a few mm or submicron size (NP), preferably in its native state, will be evaluated and established. The latter will be carried out in close collaboration with WG4 to establish novel nanospectroscopic and masspetrometric approaches as a tool for this so-far predominantly uncharted field. Providing access of standardized established, as well as newly developed, innovative approaches for users across Europe and beyond, in combination with training to enable efficient use, represents another key part of work.

WG3

Subgroups and subgroup leader

Subgroup 1 – Microscopy (optical, fluorescence)

Leader: dr. Inta Dimante-Deimantovica, Agency of Daugavpils University “Latvian Institute of Aquatic Ecology”, Latvia (inta.dimante-deimantovica@lhei.lv)

Microscopy (nanoscale)

Leader: dr. Gregor Hlawacek, Helmholtz-Zentrum Dresden-Rossendorf, Germany (g.hlawacek@thzdr.de)

Spectroscopy (IR/Raman)

Leader: dr. Maria Laura Santarelli, Sapienza Università di Roma, Italy (marialaura.santarelli@uniroma1.it)

Pyrolysis and GC/MS

Leader: dr. Laurent Lemee, Institut de Chimie des Milieux et Matériaux de Poitiers [IC2MP], France (laurent.lemee@univ-poitiers.fr)

Modelling & Data Evaluation

Leader: dr. Arianna Varrani, Institute of Geophysics Polish Academy of Sciences, Poland (avarrani@igf.edu.pl)

WG3

Meetings

WG3

Completed or ongoing activities

This Training School of 5 days had 73 participants, included 12 + 4 lectures and more than 60 poster pitch talks / poster session. Beside on-site lectures/posters/hike, and an excursion to the Research Center Rossendorf / Dresden was organized.

The study was planned and initiated in two subgroup leader meetings at 22.10.2022 and 24.04.2023 and a proposal for a study was presented at the WG 3 session at the Full Action Meeting (20.09.2023). After the Full Action Meeting a subgroup leader meeting took place at 29.09.2023 and also Thomas Meisel (WG6) participated. It was decided to do some initial tests on water heaters to check if these subjects would release enough material to be analyzed and could be suitable for a joint study.

A first pre-test exercise, known as the “Water Kettle Comparison Study”, was conducted to explore the feasibility of implementing an ILC within PRIORITY under no-budget conditions. The objective was to assess the release of microplastics during boiling processes and to compare the results obtained using various complementary analytical methods, including spectroscopic and thermal techniques.

The pre-test raised several methodological questions, such as:

  • How to design and coordinate an ILC without dedicated funding;
  • How to simplify and clarify experimental protocols;
  • Whether the particle size range produced was suitable for the analytical techniques involved;
  • And whether measurement results were reproducible within and between laboratories.

The exercise highlighted several key findings. The proposed protocol required simplification to improve clarity and ensure consistent execution among participants. A large proportion of the generated particles were smaller than 20 µm, which challenged the detection limits of some analytical techniques. As a result, reported particle counts and size distributions varied across methods, primarily due to differences in lower size thresholds and data evaluation settings.

Based on these insights, WG6 concluded that future interlaboratory studies should rely on simpler and more controlled test materials, such as microplastic suspensions of defined size and known polymer composition. These materials would allow laboratories to test identification accuracy and reproducibility under harmonized conditions, including both number- and mass-based quantification approaches.

Ultimately, the group recognized that rather than organizing new ILCs within PRIORITY itself, the most effective strategy is to collaborate with and support existing interlaboratory initiatives coordinated by metrological institutes and other established organizations. By contributing expertise, participants, and harmonized methodological recommendations, PRIORITY can best advance the shared goal of achieving robust, traceable, and internationally harmonized protocols for micro- and nanoplastic analysis.

WG3

Future/planned activities

The study was planned and initiated in two subgroup leader meetings at 22.10.2022 and 24.04.2023 and a proposal for a study was presented at the WG 3 session at the Full Action Meeting (20.09.2023). After the Full Action Meeting a subgroup leader meeting took place at 29.09.2023 and also Thomas Meisel (WG6) participated. It was decided to do some initial tests on water heaters and baby bottles to check if these subjects would release enough material to be analyzed and could be suitable for a joint study. After the pre-analysis the joint study might start.